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Abstract

Annals of Chemical Science Research

Synthesis of Piceatannol (Trans- 3,5,3’,4’-Tetrahydroxystilbene)

  • Open or CloseMixia Ma1,2 and Wenxiang Hu1,3*

    1School of Chemical and Environmental Engineering, Wuhan Institute of Technology, People’s Republic of China

    2College of Biochemical Engineering, Beijing Union University, People’s Republic of China

    3Jingdong Xianghu Microwave Chemistry Union Laboratory, Beijing tianjun Academy of Medical Sciences, People’s Republic of China

    *Corresponding author:Wenxiang Hu, School of Chemical and Environmental Engineering, Wuhan Institute of Technology, Wuhan 430073, Hubei, People’s Republic of China and Jingdong Xianghu Microwave Chemistry Union Laboratory, Beijing Tianjin Academy of Medical Sciences, Beijing 101601, People’s Republic of China

Submission: October 28, 2024;Published: November 13, 2024

DOI: 10.31031/ACSR.2024.05.000602

ISSN : 2688-8394
Volume5 Issue1

Abstract

Piceatannol was synthesized from 3,5-dimethoxyaniline through diazotization, reduction, and acetylation reactions followed by the Mizoroki-Heck coupling reaction with 3,4-dimethoxystyrene and demethylation with boron tribromide, with an overall yield of approximately 32.0%. Its structure is characterized by infra-red spectroscopy, hydrogen nuclear magnetic resonance spectroscopy, and mass spectrometry.

Keywords:Piceatannol; 3,5,3’,4’-tetrahydroxy-stilbene; Mizoroki-Heck coupling reaction; 3,4-dimethoxystyrene

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