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Abstract
Research & Development in Material Science
Fabrication of Ordered and Controlled MoOx 3D-Nanocubes by Anodization
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Kamran Ahmad1*, AttaUllah Shah2, Muhammad Bilal1, Saira Gulfam1, Rahim
Ullah2 and Zahoor Ahmad1
1Pakistan Tokamak Plasma Research Institute (PTPRI), Pakistan
2National Institute of Lasers and Optronics College (NILOP-C), Pakistan Institute of Engineering and Applied Sciences (PIEAS), Pakistan
Submission: July 07, 2022;Published: July 28, 2022
ISSN : 2576-8840Volume17 Issue3
Abstract
This study reports the formation of uniformly distributed molybdenum oxide (MoOx) nanocubes on the Mo substrate by anodization. The electrolyte contains 1 M KOH, 0.4 M NH4F and 10:1 of Ethylene Glycol (EG) and D ionized (DI) water. The Mo samples anodized for 2, 5, 7min with graphite as counter electrode in the presence of 12V respectively. The uniformly distributed cubic morphology on the surface of molybdenum is revealed by Scanning Electron Microscope (SEM). The anodization time directly controls the size of the nanocubes, increasing anodic time directly growth the nanocubes size.
Keywords: Molybdenum oxide nanocubes; Anodization; KOH and NH4F electrolyte; Anodization time
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