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Abstract
Progress in Petrochemical Science
4,4-Dimethoxy-2-butanone as 1,3-Dielectrophylic 3-Carbon Building Block: New Route for the Synthesis of Toluene, o-Xylene, Naphthalenes and Pyrimidines
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Open or Close Charanraj TP1, Ramachandra P2, Ramesh N3 and Junjappa H1*
1Chemistry Research Unit, REVA Institute of Science and Management, India
2Department of Chemistry, REVA Institute f Technology and Management, India
3Director Planning, REVA University, India
*Corresponding author: Junjappa H, Chemistry Research Unit, REVA Institute of Science & Management, Bangalore, India
Submission: July 12, 2018; Published: August 24, 2018
ISSN 2637-8035Volume2 Issue4
Abstract
4,4-dimethoxy-2-butanone 1 is shown to react with allyl magnesium chloride/allyl bromide in the presence of zinc to yield the corresponding toluene in 63% and 52% yields respectively. Similarly, crotyl bromide reacted with 1 in the presence of zinc to yield o-xylene in 32% yield. 1 was also reacted with benzyl magnesium chloride and phenyl acetonitrile to yield the corresponding naphthalenes in 53% and 61% yields respectively. The ketone 1 was reacted with guanidines to yield the corresponding pyrimidines in 58% and 66% yields respectively.
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